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Items | Acceptance criteria | Results | ||
Appearance | White crystalline power | White crystalline power | ||
Identification | A.IR spectrum consistent with that obtained with | Consistent | ||
Triclosan RS | ||||
B.The retention time of the major peak in the | Conforms | |||
chromatogram of the Assay preparation | ||||
corresponds to that in the chromatogram of the | ||||
Standard preparation, as obtained in the Assay | ||||
Water | ≤0.1% | 0.07% | ||
Residue on ignition | ≤0.1% | 0.035% | ||
Heavy metals | ≤0.002% | <0.002% | ||
Melting Point | 56-58°C | 56.3-57.5°C | ||
Related substances | Any individual impurity:≤0.1% | 0.05% | ||
Total impurities: ≤0.5% | 0.16% | |||
Assay | 97.0-103.0%(on anhydrous basis) | 99.84% | ||
Monochlorophenols | ≤50ppm | 8ppm | ||
2,4-Dichlorophenol | ≤10ppm | 3ppm | ||
1,3,7-Trichlorodibenzo-p-Dioxin | ≤0.25ppm | 0.08ppm | ||
2,8-Dichlorodibenzo-p-Dioxin | ≤0.5ppm | 0.20ppm | ||
2,8- Dichlorodibenzofuran | ≤0.25ppm | 0.06ppm | ||
2,4,8-Trichlorodibenzofuran | ≤0.5ppm | 0.24ppm | ||
2,3,7,8-Tetrachloro dibenzo-p-Dioxin | ≤1ppt | <1ppm | ||
2,3,7,8-Tetrachloro dibenzofuran | ≤1ppt | <1ppm |
Triclosan